What is the definition of a reflux? What happens to the solvent during a reflux experiment? What are

What is the definition of a reflux? What happens to the solvent during a reflux experiment? What are three characteristics of a “good” solvent to use for refluxing? You are asked to reflux a solution for one hour. At what point does the reflux time start? What is the temperature of the solution during the reflux? Should you report a melting point as a single number or a range? How are the high and low endpoints of the range determined experimentally during the melting point experiment? What is the relationship between the purity of a compound and its melting point range? Briefly describe how

»What is the definition of a reflux? What happens to the solvent during a reflux experiment? What are three characteristics of a “good” solvent to use for refluxing? You are asked to reflux a solution for one hour. At what point does the reflux time start? What is the temperature of the solution during the reflux? Should you report a melting point as a single number or a range? How are the high and low endpoints of the range determined experimentally during the melting point experiment? What is the relationship between the purity of a compound and its melting point range? Briefly describe how a rotary evaporator works. What is likely to happen if cooling water is not run through the condenser when solvent is vaporized using a rotary evaporator? That is, where is the solvent likely to end up?

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